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Old 08-29-2011, 05:46 AM   #1
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Dimethyl diallyl ammonium chloride


Monomer (two-step) synthesis process flow diagram 6DMDAAC Fig. 6ProcessofsynthesizingDMDAAC3.3 As the water samples with a certain, therefore,######## oakley sunglasses, in 34O0, 2070,1648 cm water at the three peaks. 3087cm is that: CH2 of C-H stretching vibration,true religion outlet, 1680cm is that C = C stretching vibration ,877-990cm at the C-H vibration, c-N stretching vibration is at 1015cm place. Table 6 DMDAAC element analysis results. The same water as sample, H the measured value is too large, the other value is too small. IR spectra and elemental analysis results were consistent with DMDAAC structure. This shows that the compounds really DMDAAC. By IR spectra showed no significant impurity peaks, indicating Zhen 06 a Wavenumber / m a 'map 7DMDAAC IR spectra Fig. 7FTIRdiagramofDMDAAC used in synthesis is feasible. Table 6DMDAAC element analysis Table6ChemicaldementanalysisofDMDAAC4 Conclusion technology, suitable for industrial production and so on. In order to further improve the DMDAAC yield, reduce costs needed to make a detailed study of its reaction mechanism; the impact of adverse factors on the quantitative impact of tertiary amines and tertiary amines such as quantitative analysis remains to be further explored. References: [1] CRAMMJRKR1TZFK. SynthesisofthedimethyldiaUyammt: h'nJumchloride (DMDAAC) [P]. USpatent: 542241 ~ ,1995-O6 a o6. [2] BUTLERGB. HUEYPJ. SynthesisoftheDMDAAC [P]. USpatent :3742134.1988-O5-03. [3] ZHAOHz'LUANzGAOBY'eta1. SythesisandanalysisofDMDAAC [J]. JournalofAppliedPolymerScience,tory burch outlet, 2002,84 (2) :335-342. [4] Qu Chao. PDMDAAC synthesis of a fixing agent F's process optimization Dj. Nanjing: Nanjing University. 1999. [5] YOUJN. Cydopolymeh ~ ionofdiallyaminederivativesinylsulfoxide [J]. PolymentScineee, 1967 (5) :1951-1965. [6] the right Yanmei, Hu Xuguang. Synthesis and analysis methods to improve DMDAAC [J]. Oilfield Chemistry, 1997, 14 (2) :156-161. [7] JAGERW, HAHNM, WANDREYC,herve leger sale, eta1. CyelopolymerizationkineticsofDMDAAC [J]. MacmmolSci. Chem. , 1984,herve leger toronto, A21 (5) :593-624. [8] Evergreen, Chen Ye. Han Sang En. And so on. Dimethyl diallyl ammonium chloride [J]. Environmental Science, 2000 20 (2) :168-172. [9] become increasingly flat. Diallyl amine polymer research and application in oil exploration [J]. Oilfield Chemistry, 1991,8 (3) :194-199. [10] Xu Yanli. N. N dimethyl diallyl ammonium chloride [J]. Petrochemicals. 1998,27 (7): 42 - pliers. [11] G ~ OLAMIGs, Theorganicmatterdensityestimate [J]. Chem. Educ. , 1994,71 (11) :78-8O. Author: Li Mingming (1976), male, Hebei, Shijiazhuang, teaching assistants, MA, is mainly engaged in environmental water treatment flocculant research. 5lIgm mouth d
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